GSO ISO 9396:2013
ISO 9396:1997
Gulf Standard
Current Edition
·
Approved on
01 April 2013
Plastics - Phenolic resins - Determination of the gel time of resols under specific conditions using automatic apparatus
GSO ISO 9396:2013 Files
English
4 Pages
Current Edition
Reference Language
OMR
20.31
GSO ISO 9396:2013 Scope
This International Standard specifies a method for determining the gel time of
phenolic resins at a given temperature, using automatic apparatus under specified
conditions. The test temperatures are 100 “C, 130 “C and 150 “C.
The method specified employs a plunger driven to carry out a reciprocating vertical
motion. ,
This method applies to the following types of phenolic resin:
- liquid resols
- solid resols with low melting points
Powdered resins with a short gel time, such as mixtures of novolak and
hexamethylenetetramine, do not lend themselves to this type of determination. Such
resins crosslink as soon as fusion starts and become too viscous in the test tube to give
meaningful results. Resins containing large amounts of a solvent with a low boiling point
are especially unsuitable for this type of determination. With such resins, a boiling and
distillation process takes place as the resin hardens.
It might be of interest to determine the time taken for the resin to gel in the presence
of a catalyst. The catalyst shall be added in well defined proportions. The type of
catalyst used and its treatment shall be stated in the test report.
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